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Thesis

Synthetic aspects of organosulphur chemistry

Abstract:

The thesis is concerned with approaches to substituted 2-phenyl- 1,3-oxathiolans and their cycloreversion to olefins.

2-(α-Methoxybenzylthio)acetophenone (l) was prepared by in situ alkylation of the thiolate generated by aminolysis of 0-ethyl-S-phenacyldithiocarbonate with α-chlorobenzyl methyl ether. Reduction of (l) with lithium aluminium hydride gave 2-(α-methoxybenzylthio)—1— phenylethanol which cyclised in the presence of p-toluenesulphonic acid to give 2,5-dipheny... Expand abstract

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Institution:
University of Oxford
Division:
MPLS
Role:
Author

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Role:
Supervisor
Role:
Supervisor
Publication date:
1984
Type of award:
DPhil
Level of award:
Doctoral
Awarding institution:
University of Oxford
Language:
English
Subjects:
UUID:
uuid:0933318b-efc3-4b4d-9453-2cfdaeed07c1
Local pid:
td:603839469
Source identifiers:
603839469
Deposit date:
2015-02-10

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