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3D printed silica-gelatin hybrid scaffolds of specific channel sizes promote collagen Type II, Sox9 and Aggrecan production from chondrocytes

Abstract:
Inorganic/organic hybrids have co-networks of inorganic and organic components, with the aim of obtaining synergy of the properties of those components. Here, a silica-gelatin sol-gel hybrid "ink" was directly 3D printed to produce 3D grid-like scaffolds, using a coupling agent, 3-glycidyloxypropyl)trimethoxysilane (GPTMS), to form covalent bonds between the silicate and gelatin co-networks. Scaffolds were printed with 1 mm strut separation, but the drying method affected the final architecture and properties. Freeze drying produced <40 μm struts and large ~700 μm channels. Critical point drying enabled strut consolidation, with ~160 μm struts and ~200 μm channels, which improved mechanical properties. This architecture was critical to cellular response: when chondrocytes were seeded on the scaffolds with 200 μm wide pore channels in vitro, collagen Type II matrix was preferentially produced (negligible amount of Type I or X were observed), indicative of hyaline-like cartilaginous matrix formation, but when pore channels were 700 μm wide, Type I collagen was prevalent. This was supported by Sox9 and Aggrecan expression. The scaffolds have potential for regeneration of articular cartilage regeneration, particularly in sports medicine cases.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1016/j.msec.2021.111964

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Funder identifier:
https://ror.org/03x94j517
Grant:
MR/R025673/1
MR/R015651/1


Publisher:
Elsevier
Journal:
Materials Science and Engineering: C More from this journal
Volume:
123
Article number:
111964
Place of publication:
Netherlands
Publication date:
2021-02-12
Acceptance date:
2021-02-08
DOI:
EISSN:
1873-0191
ISSN:
0928-4931
Pmid:
33812592

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