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A spectrometer designed for 6.7 and 14.1 T DNP-enhanced solid-state MAS NMR using quasi-optical microwave transmission.

Abstract:

A Dynamic Nuclear Polarisation (DNP) enhanced solid-state Magic Angle Spinning (MAS) NMR spectrometer operating at 6.7 T is described and demonstrated. The 187 GHz TE(13) fundamental mode of the FU CW VII gyrotron is used as the microwave source for this magnetic field strength and 284 MHz (1)H DNP-NMR. The spectrometer is designed for use with microwave frequencies up to 395 GHz (the TE(16) second-harmonic mode of the gyrotron) for DNP at 14.1T (600 MHz (1)H NMR). The pulsed microwave output...

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Publication status:
Published

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Publisher copy:
10.1016/j.jmr.2011.12.006

Authors


Takahashi, H More by this author
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Journal:
Journal of magnetic resonance (San Diego, Calif. : 1997)
Volume:
215
Pages:
1-9
Publication date:
2012-02-05
DOI:
EISSN:
1096-0856
ISSN:
1090-7807
URN:
uuid:fd4adffb-27c2-4130-b88e-a10418a0775d
Source identifiers:
245918
Local pid:
pubs:245918

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