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Ultra-high resolution 17O solid-state NMR spectroscopy of biomolecules: a comprehensive spectral analysis of monosodium L-glutamate·monohydrate.

Abstract:

Monosodium L-glutamate monohydrate, a multiple oxygen site (eight) compound, is used to demonstrate that a combination of high-resolution solid-state NMR spectroscopic techniques opens up new possibilities for (17)O as a nuclear probe of biomolecules. Eight oxygen sites have been resolved by double rotation (DOR) and multiple quantum (MQ) NMR experiments, despite the (17)O chemical shifts lying within a narrow shift range of <50 ppm. (17)O DOR NMR not only provides high sensitivity and spe...

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Publication status:
Published

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Publisher copy:
10.1039/c1cp20629j

Authors


More by this author
Institution:
University of Oxford
Division:
MSD
Department:
Biochemistry
Role:
Author
Journal:
Physical chemistry chemical physics : PCCP More from this journal
Volume:
13
Issue:
26
Pages:
12213-12224
Publication date:
2011-07-01
DOI:
EISSN:
1463-9084
ISSN:
1463-9076
Language:
English
Keywords:
Pubs id:
pubs:164242
UUID:
uuid:f4e52001-0d58-4f55-8114-6ae0c879995d
Local pid:
pubs:164242
Source identifiers:
164242
Deposit date:
2012-12-19

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