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Crystal structures of [XnE]+[(η7-C7H7)Mo(CO)2GaI3]- (XnE = (thf)4Li, Cy3PH)

Abstract:
The crystal structures of [XnE]+[(η7-C7H7)Mo(CO)2GaI3]- [XnE = (C4H8O)4Li (1), (C6H11)3PH (2)] are reported, revealing: (1) monoclinic, P21/c, a = 11.2388(1), b = 17.3201(3), c = 17.5473(2)Å, β = 101.623(1)°, Z = 4, R = 0.038 and wR2 = 0.090 for 7614 observed reflections [I>2σ(I)]; (2) monoclinic, P21/n, a = 9.2979(5), b = 18.4632(8), c = 19.9789(9)Å, β = 99.325(3)°, Z = 4, R = 0.073 and wR2 = 0.184 for 5554 observed reflections [I > 2σ (I)]. 2007 © The Japan Society for Analytical Chemistry.

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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
Journal:
Analytical Sciences: X-ray Structure Analysis Online More from this journal
Volume:
23
Issue:
11
Publication date:
2007-01-01
EISSN:
1348-2238
Language:
English
Pubs id:
pubs:130685
UUID:
uuid:f2df7184-a068-4879-ac30-b6c28e472135
Local pid:
pubs:130685
Source identifiers:
130685
Deposit date:
2012-12-19

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