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2-azido-(R)-3,5-O-benzylidene-2-deoxy-2-C-methyl-D-xylono-1,4-lactone [(2S, 4aR, 7R,7aR)-7-azido-7-methyl-2-phenyldihydro-4H-furo[3,2-d][1,3]dioxin6(4aH)-one]

Abstract:
The unknown relative configurations in the title compound, C13H13N3O4, of the acetal carbon and of the quaternary carbon bearing the azide were determined by X-ray crystallographic analysis; the absolute configuration was defined by the use of 2-C-methyl-D-lyxonolactone as a starting material. There are two mol-ecules in the asymmetric unit (Z′ = 2). © 2007 International Union of Crystallography. All rights reserved.
Publication status:
Published

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Publisher copy:
10.1107/S1600536807014560

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Role:
Author
Journal:
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
Volume:
63
Issue:
5
Pages:
O2168-O2170
Publication date:
2007-05-05
DOI:
EISSN:
1600-5368
ISSN:
1600-5368
URN:
uuid:ece2135f-43ec-467f-b71b-f5661b9c7c41
Source identifiers:
40424
Local pid:
pubs:40424
Language:
English

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