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Lanthanide Structures, Coordination, and Extraction Investigations of a 1,3-Bis(diethyl amide)-Substituted Calix[4]arene Ligand.

Abstract:

The synthesis and structure determinations of lanthanum, samarium, ytterbium, and lutetium complexes of 5,11,17,23-tetra-tert-butyl-25,27-bis((diethylcarbamoyl)methoxy)-26,28-dihydroxycalix[4]arene (L) are described. The four structures display similar characteristics with the trivalent lanthanide cation being encapsulated in an eight-coordinate oxygen environment, consisting of six oxygens from the calixarene, a water molecule, and unidentate picrate for lanthanum [La(L-2H)(picrate)(H(2)O)];...

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Publication status:
Published

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Publisher copy:
10.1021/ic9512441

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Leeson, PB More by this author
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Journal:
Inorganic chemistry
Volume:
35
Issue:
8
Pages:
2202-2211
Publication date:
1996-04-05
DOI:
EISSN:
1520-510X
ISSN:
0020-1669
URN:
uuid:e9d2aefc-eae8-491a-9d82-ab99eda3a59c
Source identifiers:
31970
Local pid:
pubs:31970
Language:
English

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