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Electro-oxidation of hydrazine shows Marcusian electron transfer kinetics

Abstract:
Although hydrazine (N2H4) oxidation in an electrochemical environment has been of great interest for years its intrinsic electron transfer kinetics remain uncertain. We report that the phenomenological Butler-Volmer (BV) theory is not appropriate for interpreting the process of hydrazine oxidation for which an astonishingly wide range of transfer coefficients, Tafel slopes and diffusion coefficient have been previously reported. Rather Tafel analysis for voltammetry recorded at Glassy Carbon (GC) electrodes reveals a strong potential dependence of the anodic transfer coefficient, consistent with the symmetric Marcus-Hush (sMH) theory. According to the relationship β=(λ+FE0f)/(2λ-F/2λe), the reorganization energy (0.35 ± 0.07 eV) and an approximate formal potential of the rate-determining first electron transfer were successfully extracted from the voltammetric responses.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1007/s11426-020-9889-1

Authors


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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Chemistry
Role:
Author


Publisher:
Springer
Journal:
Science China Chemistry More from this journal
Volume:
64
Issue:
2
Pages:
322–329
Publication date:
2020-12-02
Acceptance date:
2020-10-15
DOI:
EISSN:
1869-1870
ISSN:
1674-7291


Language:
English
Keywords:
Pubs id:
1137795
Local pid:
pubs:1137795
Deposit date:
2020-10-15

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