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Li0.7NbS2: structural effects of increased alkali metal content

Abstract:

Crystals of lithium niobium disulfide [LiyNbS2; y = 0.70 (9)] have been prepared by separated reactants metathesis (SRM) at 1073 K. Single-crystal data collected at reduced temperature [150 (2) K] indicate that the compound is isostructural with Li0.63NbS2 [Salyer, Barker, Blake, Gregory and Wilson (2003). Acta Cryst. C59, i4-i6], crystallizing in the hexagonal space group P63/mmc (No. 194). Li 0.7NbS2 shows an expansion of both the a and c lattice parameters when compared with previously rep...

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Publication status:
Published

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Publisher copy:
10.1107/S1600536803014855

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Role:
Author
Journal:
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
Volume:
59
Issue:
8
Pages:
I112-I115
Publication date:
2003-08-05
DOI:
EISSN:
1600-5368
ISSN:
1600-5368
URN:
uuid:e9b52855-eb6a-498c-8306-4c957437cd6f
Source identifiers:
104479
Local pid:
pubs:104479
Language:
English

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