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Complete (1)H resonance assignment of beta-maltose from (1)H-(1)H DQ-SQ CRAMPS and (1)H (DQ-DUMBO)-(13)C SQ refocused INEPT 2D solid-state NMR spectra and first principles GIPAW calculations.

Abstract:

A disaccharide is a challenging case for high-resolution (1)H solid-state NMR because of the 24 distinct protons (14 aliphatic and 10 OH) having (1)H chemical shifts that all fall within a narrow range of approximately 3 to 7 ppm. High-resolution (1)H (500 MHz) double-quantum (DQ) combined rotation and multiple pulse sequence (CRAMPS) solid-state NMR spectra of beta-maltose monohydrate are presented. (1)H-(1)H DQ-SQ CRAMPS spectra are presented together with (1)H (DQ)-(13)C correlation spectr...

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Publication status:
Published

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Publisher copy:
10.1039/c001290d

Authors


Webber, AL More by this author
Griffin, JM More by this author
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Journal:
Physical chemistry chemical physics : PCCP
Volume:
12
Issue:
26
Pages:
6970-6983
Publication date:
2010-07-05
DOI:
EISSN:
1463-9084
ISSN:
1463-9076
URN:
uuid:e96e2318-6cc2-42c3-a5ed-47d58147f6c8
Source identifiers:
178970
Local pid:
pubs:178970
Language:
English

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