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2,5-Anhydro-N-benzyl-2-C-methyl-D-arabinonamide [(2S,3R,4R)-N-benzyl-3,4-dihydroxy-2-methyltetrahydrofuran-2-carboxamide]

Abstract:

The size of the ring and relative configuration of the chiral centres in the title compound, C13H17NO4, formed by the preferential formation of the hindered five-membered ring tetrahydrofuran rather than the expected three-membered ring epoxide, was established by X-ray crystallographic analysis; the absolute configuration was determined by the use of 2-C-methyl-D-arabinono-lactone as the starting material. The crystal structure consists of hydrogen-bonded layers lying with their hydrophobic ...

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Publication status:
Published

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Publisher copy:
10.1107/S1600536806055322

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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Organic Chemistry
Role:
Author
Journal:
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
Volume:
63
Issue:
2
Pages:
O574-O576
Publication date:
2007-02-01
DOI:
EISSN:
1600-5368
ISSN:
1600-5368
Source identifiers:
40268
Language:
English
Pubs id:
pubs:40268
UUID:
uuid:cfdfb83e-61c1-47a0-88c1-b7802b1728ca
Local pid:
pubs:40268
Deposit date:
2012-12-19

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