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[Cu4@E18]4– (E = Sn, Pb): fused derivatives of endohedral stannaspherene and plumbaspherene

Abstract:

We report the synthesis of two new cluster anions, [Cu4@E18]4– (E = Sn, Pb), in which a Cu4 subunit is incorporated into a continuous E18 tetrel cage. Both anions are characterized by X-ray crystallography and mass spectrometry, complemented by quantum-chemical calculations that highlight the relationships to known Zintl clusters, including the stannaspherenes and plumbaspherenes [M@Sn12]q and [M@Pb12]q, the Matryoshka bronze [Sn@Cu12@Sn20]12–, and also [Pd2@E′18]4– (E′ = Ge, Sn).

Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1021/jacs.0c04815

Authors


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Role:
Author
ORCID:
0000-0002-6602-6532
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Role:
Author
ORCID:
0000-0002-0368-0801
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Role:
Author
ORCID:
0000-0001-7407-3446
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Role:
Author
ORCID:
0000-0001-9647-8807
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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
ORCID:
0000-0002-8991-1921


Publisher:
American Chemical Society
Journal:
Journal of the American Chemical Society More from this journal
Volume:
142
Issue:
31
Pages:
13288-13293
Publication date:
2020-07-20
Acceptance date:
2020-07-20
DOI:
EISSN:
1520-5126
ISSN:
0002-7863


Language:
English
Keywords:
Pubs id:
1122978
Local pid:
pubs:1122978
Deposit date:
2020-07-31

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