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Heterometallic lanthanide complexes with site-specific binding that enable simultaneous visible and NIR-emission

Abstract:

Macrocyclic lanthanide complexes have become widely developed due to their distinctive luminescence characteristics and wide range of applications in biological imaging. However, systems with sufficient brightness and metal selectivity can be difficult to produce on a molecular scale. Presented herein is the stepwise introduction of differing lanthanide ions in a bis-DO3A/DTPA scaffold to afford three trinuclear bimetallic [Ln2Ln’] lanthanide complexes with site-specific, controlled binding [(Yb2Tb), (Eu2Tb), (Yb2Eu)]. The complexes display simultaneous emission from all LnIII centers across the visible (TbIII, EuIII) and near infra-red (YbIII) spectrum when excited via phenyl ligand sensitization at a wide range of temperatures and are consequently of interest for exploiting imaging in the near infra-red II biological window. Analysis of lifetime data over a range of excitation regimes reveals intermetallic communication between TbIII and EuIII centers and further develops the understanding of multimetallic lanthanide complexes.

Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.3389/fchem.2023.1232690

Authors

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Role:
Author
ORCID:
0000-0001-9429-9768
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Chemistry Research Laboratory
Oxford college:
Keble College
Role:
Author
ORCID:
0000-0003-1878-5857


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Funder identifier:
https://ror.org/00cwqg982
Grant:
BB/M011208/1


Publisher:
Frontiers Media
Journal:
Frontiers in Chemistry More from this journal
Volume:
11
Article number:
1232690
Publication date:
2023-07-31
Acceptance date:
2023-07-17
DOI:
EISSN:
2296-2646
Pmid:
37583568


Language:
English
Keywords:
Pubs id:
1510227
Local pid:
pubs:1510227
Deposit date:
2025-03-28
ARK identifier:

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