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Pb-207 NMR chemical shifts of lead tetracarboxylates

Abstract:

207Pb NMR spectroscopy was used to investigate 20 lead(IV) tetracarboxylates both in solution and in the solid state by cross-polarization magic angle spinning (CP/MAS) NMR. There is generally good correlation between isotropic chemical shifts in the solid state and those in solution. Multiple CP/MAS NMR isotropic resonances are observed for three of the compounds and are interpreted in terms of multiple molecules in the crystallographic asymmetric unit. From an analysis of the range of, and ...

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Publication status:
Published

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Authors


Buston, JEH More by this author
More by this author
Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Bretherton, JL More by this author
More by this author
Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
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Journal:
MAGNETIC RESONANCE IN CHEMISTRY
Volume:
39
Issue:
2
Pages:
68-76
Publication date:
2001-02-05
DOI:
EISSN:
1097-458X
ISSN:
0749-1581
URN:
uuid:a562dfbb-8f90-4f43-a7d4-71b88b975a56
Source identifiers:
37731
Local pid:
pubs:37731

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