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Composition-dependent transition from spin glass to ferrimagnet in CaLa2Ni2-xCuxWO9 (0 ≤ x ≤ 0.5)

Abstract:
Polycrystalline samples of the monoclinic perovskites CaLa2Ni2-xCuxWO9 (x = 0.25 and 0.5) have been prepared and characterised by neutron diffraction and magnetometry. The Ni2+, Cu2+ and W6+ cations are partially ordered over two crystallographically-distinct six-coordinate sites such that one is ∼63% occupied by W6+ and both are occupied by Ni2+ and Cu2+ in a ratio of (2-x):x. The composition x = 0.25 behaves as a spin glass below 35 K whereas x = 0.5 is ferrimagnetic below 120 K with an ordered moment of 0.774(5) μB per magnetic cation. The atomic moments order in a G-type pattern and the imbalance in the number of magnetic cations on the two sites results in a net magnetisation.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1016/j.jssc.2020.121388

Authors

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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author


Publisher:
Elsevier
Journal:
Journal of Solid State Chemistry More from this journal
Volume:
287
Issue:
July 2020
Article number:
121388
Publication date:
2020-04-14
Acceptance date:
2020-04-09
DOI:
ISSN:
0022-4596


Language:
English
Keywords:
Pubs id:
1100040
Local pid:
pubs:1100040
Deposit date:
2020-04-14
ARK identifier:

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