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Chemoselective carbene insertion into the N−H bonds of NH3·H2O

Abstract:
O and enables the generation of electrophilic silver carbene. Water promotes subsequent [1,2]-proton shift to generate N-H insertion products with high chemoselectivity. The result of the reaction is the coupling of an inorganic nitrogen source with either diazo compounds or N-triftosylhydrazones to produce useful primary amines. Further investigations elucidate the reaction mechanism and the origin of chemoselectivity.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1038/s41467-022-35394-z

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Role:
Author
ORCID:
0000-0001-9951-8675
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Role:
Author
ORCID:
0000-0001-8872-2777
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Role:
Author
ORCID:
0000-0003-3546-2961
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Role:
Author
ORCID:
0000-0001-9836-1442
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Role:
Author
ORCID:
0000-0003-1530-9409


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Funder identifier:
10.13039/501100001809
Grant:
21871043
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Funder identifier:
10.13039/501100011789
Grant:
20200801065GH


Publisher:
Nature Research
Journal:
Nature Communications More from this journal
Volume:
13
Issue:
1
Pages:
7649-7649
Article number:
7649
Publication date:
2022-12-10
DOI:
EISSN:
2041-1723
ISSN:
2041-1723


Language:
English
Keywords:
Pubs id:
1314648
Local pid:
pubs:1314648
Source identifiers:
W4311931393
Deposit date:
2026-04-30
ARK identifier:
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