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Tuning the selectivity of NH3 oxidation via cooperative electronic interactions between platinum and copper sites

Abstract:
Selective catalytic oxidation (SCO) of NH3 to N2 is one of the most effective methods used to eliminate NH3 emissions. However, achieving high conversion over a wide operating temperature range while avoiding over-oxidation to NOx remains a significant challenge. Here, we report a bi-metallic surficial catalyst (PtSCuO/Al2O3) with improved Pt atom efficiency that overcomes the limitations of current catalysts. It achieves full NH3 conversion at 250°C with a weight hourly space velocity of 600 ml NH3·h-1·g-1, which is 50°C lower than commercial Pt/Al2O3, and maintains high N2 selectivity through a wide temperature window. Operando XAFS studies reveal that the surface Pt atoms in PtSCuO/Al2O3 enhance the redox properties of the Cu species, thus accelerating the Cu2+ reduction rate and improving the rate of the NH3-SCO reaction. Moreover, a synergistic effect between Pt and Cu sites in PtSCuO/Al2O33 contributes to the high selectivity by facilitating internal selective catalytic reduction.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1038/s41467-024-54820-y

Authors


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Role:
Author
ORCID:
0000-0002-5324-9534
More by this author
Role:
Author
ORCID:
0000-0002-3820-010X
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Role:
Author
ORCID:
0000-0001-6451-4738


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Funder identifier:
https://ror.org/0439y7842
Grant:
EP/X022986/1


Publisher:
Springer Nature
Journal:
Nature Communications More from this journal
Volume:
16
Issue:
1
Article number:
26
Publication date:
2025-01-02
Acceptance date:
2024-11-20
DOI:
EISSN:
2041-1723


Language:
English
Pubs id:
2074385
Local pid:
pubs:2074385
Deposit date:
2025-01-06

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