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Molecular sensitised probe for amino acid recognition within peptide sequences

Abstract:
The combination of low-temperature scanning tunnelling microscopy with a mass-selective electro-spray ion-beam deposition established the investigation of large biomolecules at nanometer and sub-nanometer scale. Due to complex architecture and conformational freedom, however, the chemical identification of building blocks of these biopolymers often relies on the presence of markers, extensive simulations, or is not possible at all. Here, we present a molecular probe-sensitisation approach addressing the identification of a specific amino acid within different peptides. A selective intermolecular interaction between the sensitiser attached at the tip-apex and the target amino acid on the surface induces an enhanced tunnelling conductance of one specific spectral feature, which can be mapped in spectroscopic imaging. Density functional theory calculations suggest a mechanism that relies on conformational changes of the sensitiser that are accompanied by local charge redistributions in the tunnelling junction, which, in turn, lower the tunnelling barrier at that specific part of the peptide.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1038/s41467-023-43844-5

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Role:
Author
ORCID:
0000-0002-2252-322X
More by this author
Role:
Author
ORCID:
0000-0001-5485-4536


Publisher:
Springer Nature
Journal:
Nature Communications More from this journal
Volume:
14
Issue:
1
Article number:
8335
Place of publication:
England
Publication date:
2023-12-14
Acceptance date:
2023-11-21
DOI:
EISSN:
2041-1723
Pmid:
38097575


Language:
English
Pubs id:
1588745
Local pid:
pubs:1588745
Deposit date:
2024-01-17

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