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High-resolution imaging of complex crack chemistry in reactor steels by NanoSIMS

Abstract:

High-resolution analysis using a Cameca NanoSIMS 50 has been used to map the oxide chemistry in intergranular cracks in stainless steels. The technique has proven ideal for this type of sample, as it is able to discern between the different oxide layers and clarify the role of minor segregants such as boron and sulphur. Results are compared with analysis of the same sample by scanning auger microscopy and its interpretation discussed. The short time required to prepare and examine multiple re...

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Publication status:
Published

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Publisher copy:
10.1016/j.jnucmat.2007.07.009

Authors


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Institution:
University of Oxford
Division:
MPLS
Department:
Materials
Role:
Author
Journal:
JOURNAL OF NUCLEAR MATERIALS More from this journal
Volume:
374
Issue:
1-2
Pages:
61-68
Publication date:
2008-02-29
DOI:
ISSN:
0022-3115
Language:
English
Pubs id:
pubs:16488
UUID:
uuid:4bfdc9bc-f37b-484d-99c3-87317eaead7a
Local pid:
pubs:16488
Source identifiers:
16488
Deposit date:
2012-12-19

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