Journal article
Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)
- Abstract:
- The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump-probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.
- Publication status:
- Published
- Peer review status:
- Peer reviewed
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(Preview, Version of record, pdf, 2.5MB, Terms of use)
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- Publisher copy:
- 10.1107/s1600577521002551
Authors
- Publisher:
- International Union of Crystallography
- Journal:
- Journal of Synchrotron Radiation More from this journal
- Volume:
- 28
- Issue:
- 3
- Pages:
- 688-706
- Place of publication:
- United States
- Publication date:
- 2021-04-14
- Acceptance date:
- 2021-03-08
- DOI:
- EISSN:
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1600-5775
- ISSN:
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0909-0495
- Pmid:
-
33949979
- Language:
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English
- Keywords:
- Pubs id:
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1178078
- Local pid:
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pubs:1178078
- Deposit date:
-
2023-07-10
Terms of use
- Copyright holder:
- Liermann et al
- Copyright date:
- 2021
- Rights statement:
- ©2021 The Author(s). This is an Open Access article under the CC BY 4.0 license.
- Licence:
- CC Attribution (CC BY)
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