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Block poly(carbonate-ester) ionomers as high-performance and recyclable thermoplastic elastomers

Abstract:
Thermoplastic elastomers based on polyesters/carbonates have the potential to maximize recyclability, degradability and renewable resource use. However, they often underperform and suffer from the familiar trade-off between strength and extensibility. Herein, we report well-defined reprocessable poly(ester-b-carbonateb- ester) elastomers with impressive tensile strengths (60 MPa), elasticity (>800%) and recovery (95%). Plus, the ester/carbonate linkages are fully degradable and enable chemical recycling. The superior performances are attributed to three features: (1) Highly entangled soft segments; (2) fully reversible strain-induced crystallization and (3) precisely placed Zn(II)-carboxylates dynamically crosslinking the hard domains. The one-pot synthesis couples controlled cyclic monomer ring-opening polymerization and alternating epoxide/anhydride ring-opening copolymerization. Easy conversion to ionomers is achieved using vinyl-substituted epoxides with phthalic anhydride.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1002/anie.202210748

Authors


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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Oxford college:
Trinity College
Role:
Author
ORCID:
0000-0002-0734-1575


Publisher:
Wiley
Journal:
Angewandte Chemie International Edition More from this journal
Volume:
61
Issue:
47
Article number:
e202210748
Publication date:
2022-10-21
Acceptance date:
2022-09-29
DOI:
EISSN:
1521-3773
ISSN:
1433-7851


Language:
English
Keywords:
Pubs id:
1281480
Local pid:
pubs:1281480
Deposit date:
2022-10-05

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