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Electrochemistry in tetrahydrofuran and at low temperature: protocol, procedures and methods

Abstract:

This review describes the protocol, procedures and methods for electrochemical studies in THF and at low temperature that have been developed in the course of the last 5 years in our laboratory. Electrochemical studies in THF benefit from a large accessible potential window. In practice, it is however necessary to avoid the presence of humidity in the electrochemical cell. A specific reference electrode had to be designed for those measurements. Microelectrodes, the voltammetric response of w...

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Publication status:
Published

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Publisher copy:
10.1002/poc.1574

Authors


Kershaw, NM More by this author
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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
More by this author
Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Physical and Theoretical Chem
Journal:
JOURNAL OF PHYSICAL ORGANIC CHEMISTRY
Volume:
22
Issue:
12
Pages:
1136-1141
Publication date:
2009-12-05
DOI:
EISSN:
1099-1395
ISSN:
0894-3230
URN:
uuid:43eb8f15-8ea8-4b44-800b-28a4c262192d
Source identifiers:
41483
Local pid:
pubs:41483

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