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Stereochemical Assignment of Substituted 2-Aminobicyclo[3.1.0]hexane and 2-Aminobicyclo[5.1.0]octane Derivatives via Single Crystal X-ray Diffraction

Abstract:

Crystals of benzyl (RS,RS,RS)-7-phenylbicyclo[5.1.0]octan-2-ylcarbamate 9 and (RS,RS,RS)-N-[3′-(4′-methylpiperazin-1′-yl)propyl]-N-{5- (4‴-cyanophenyl)bicyclo[3.1.0]hexan-2-yl}amine dihydrochloride 10•2HCl were synthesised and single crystal X-ray diffraction was used to establish unambiguously the relative configurations within these structures. Compound 9 crystallizes in the orthorhombic space group P2 1 2 1 2 1 with cell parameters of a = 6.85340(10) Å, b = 9.8732(2) Å, c = 27.5407(6) Å, V...

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Publication status:
Published

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Publisher copy:
10.1007/s10870-011-0034-6

Authors


More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Organic Chemistry
Role:
Author
Journal:
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY More from this journal
Volume:
41
Issue:
7
Pages:
1007-1012
Publication date:
2011-07-01
DOI:
EISSN:
1572-8854
ISSN:
1074-1542
Language:
English
Keywords:
Pubs id:
pubs:162210
UUID:
uuid:23e36f46-9d71-4e95-9f00-8f28e6d0e5e3
Local pid:
pubs:162210
Source identifiers:
162210
Deposit date:
2012-12-19

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