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Journal article

High-resolution mass spectrometry of small molecules bound to membrane proteins

Abstract:
Small molecules are known to stabilize membrane proteins and to modulate their function and oligomeric state, but such interactions are often hard to precisely define. Here we develop and apply a high-resolution, Orbitrap mass spectrometry–based method for analyzing intact membrane protein–ligand complexes. Using this platform, we resolve the complexity of multiple binding events, quantify small molecule binding and reveal selectivity for endogenous lipids that differ only in acyl chain length.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1038/nmeth.3771

Authors


More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Physical & Theoretical Chem
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Physical & Theoretical Chem
Role:
Author
Publisher:
Springer Nature
Journal:
Nature methods More from this journal
Volume:
13
Issue:
4
Pages:
333-336
Publication date:
2016-04-01
Acceptance date:
2016-01-13
DOI:
EISSN:
1548-7105
ISSN:
1548-7091
Pmid:
26901650
Language:
English
Keywords:
Pubs id:
pubs:605932
UUID:
uuid:1a81bf2a-17d1-4bb0-bc7b-7cdb1345b9dc
Local pid:
pubs:605932
Source identifiers:
605932
Deposit date:
2016-12-09

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