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TEM investigations of industrial platinum on graphite catalyst systems: Image processing and particle morphology

Abstract:
Industrial platinum on graphite catalysts, prepared by salt deposition from aqueous solution, have been examined using transmission electron microscopy. The resulting micrographs show a mixture of dendritic metal islands, and smaller (1-4nm diameter) spherical islands. An image processing technique has been developed to subtract the graphite backgrounds, allowing the images to be made binary. The dendricity of a particle is then characterised by the formfactor, a measure derived from the TEM images, thus a quantitative comparison between the different, highly irregular, industrial catalyst samples is made feasible.
Publication status:
Published

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Institution:
University of Oxford
Division:
MPLS
Department:
Materials
Role:
Author


Journal:
ELECTRON MICROSCOPY AND ANALYSIS 2001 More from this journal
Issue:
168
Pages:
421-424
Publication date:
2001-01-01
Event title:
Conference of the Electron-Microscopy-and Analysis-Group
ISSN:
0951-3248
ISBN:
0750308125


Pubs id:
pubs:12577
UUID:
uuid:11362033-716a-4b10-b03c-e3eaff85f4f7
Local pid:
pubs:12577
Source identifiers:
12577
Deposit date:
2012-12-19
ARK identifier:

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