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Synthesis and structural studies of gallium(III) and indium(III) complexes of 2-acetylpyridine thiosemicarbazones

Abstract:

Four 2-acetylpyridine 4N-alkyl thiosemicarbazones, and their Ga(III) and In(III) complexes have been prepared and characterised by fluorescence, UV-Vis, IR, 1H and 13C NMR spectroscopy, mass spectrometry and X-ray crystallographic analysis. Comparison of the crystal structures gave an insight into the nature of the complexes formed, demonstrating a preference for [ML2]+ type complexes with gallium and [MLX3] species with indium. Stability studies on two candidates indicated that complex [InL3...

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Publication status:
Published

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Publisher copy:
10.1016/j.ica.2009.10.020

Authors


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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
Journal:
INORGANICA CHIMICA ACTA More from this journal
Volume:
363
Issue:
6
Pages:
1140-1149
Publication date:
2010-04-05
DOI:
ISSN:
0020-1693
Language:
English
Keywords:
Pubs id:
pubs:117166
UUID:
uuid:0b4ad534-253e-4730-9357-c54b182e1426
Local pid:
pubs:117166
Source identifiers:
117166
Deposit date:
2012-12-19

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