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Voltammetric reduction of perinaphthenone in aqueous and non-aqueous media: An electrochemical ESR investigation

Abstract:

The electrochemical reduction of perinaphthenone on solid electrodes in aqueous and non-aqueous media is reported and paramagnetic species formed are characterised by use of electrochemical ESR, employing a tubular flow cell. In aqueous ethanol a single electron reduction process generates the radical anion which is protonated at pH < 9, as indicated by the shift of the voltammetric wave with pH. Observed ESR spectra are presented and signal intensity measurements show that the neutral rad...

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Publication status:
Published

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Physical and Theoretical Chem
Journal:
JOURNAL OF ELECTROANALYTICAL CHEMISTRY
Volume:
589
Issue:
1
Pages:
128-138
Publication date:
2006-04-01
DOI:
ISSN:
0022-0728
URN:
uuid:0a8f8b93-c61e-402b-90da-ec43c811053d
Source identifiers:
39928
Local pid:
pubs:39928

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