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Synthesis, characterisation and molecular structures of the closo and pseudocloso heptamethylindenyl carbarhodaboranes 1-Ph-3-(eta-C(9)Me(7))-3,1,2-closo-RhC2B9H10 and 1,2-Ph(2)-3-(eta-C(9)Me(7))-3,1,2-pseudocloso-RhC2B9H9. Experimental assignment of the B-11 NMR spectrum of a pseudocloso carbametallaborane

Abstract:

Title full: Synthesis, characterisation and molecular structures of the closo and pseudocloso heptamethylindenyl carbarhodaboranes 1-Ph-3-(η-C9Me7)-3,1,2-closo-RhC2B 9H10 and 1,2-Ph2-3-(η-C9Me 7)-3,1,2-pseudocloso-RhC2B9H9. Experimental assignment of the 11B NMR spectrum of a pseudocloso carbametallaborane. The reaction between [{RhCl2(η-C9Me7)}2] and Tl2[7-Ph-8-R-7,8-nido-C2B9H9] (R = H or Ph) in CH2Cl2 afforded the heptamethylindenyl carbarhodaboranes 1-Ph-3-(η-C9Me7)-3,1,2-RhC2B 9H10 1 and...

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Publication status:
Published

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Publisher copy:
10.1039/dt9960000335

Authors


Gradler, U More by this author
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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Journal:
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS
Issue:
3
Pages:
335-342
Publication date:
1996-02-07
DOI:
EISSN:
1364-5447
ISSN:
0300-9246
URN:
uuid:09c4d172-5980-4a0c-92c6-43b8297c867f
Source identifiers:
51745
Local pid:
pubs:51745
Language:
English

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