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A general route to alkylene-, arylene-, or benzylene-bridged ditin hexachlorides and hexaalkynides

Abstract:
The preparation of alkylene-, arylene-, or benzylene-bridged ditin hexachlorides in high yields from the reaction of the corresponding hexacyclohexylated compounds with tin tetrachloride is described. The tetragonal geometry of the tin atom of 1,4-bis(trichlorostannyl)-butane in the solid state indicates that no intramolecular or intermolecular interaction involving either end of the molecule exists in this compound. The ditin hexachlorides were successfully transformed in the corresponding hexaalkynides, precursors of hybrid materials.
Publication status:
Published

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Publisher copy:
10.1021/om0202468

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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
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Journal:
ORGANOMETALLICS
Volume:
21
Issue:
22
Pages:
4590-4594
Publication date:
2002-10-28
DOI:
EISSN:
1520-6041
ISSN:
0276-7333
Source identifiers:
51218
Language:
English
Pubs id:
pubs:51218
UUID:
uuid:0895948a-f98f-40a6-81da-22b13c3e5e48
Local pid:
pubs:51218
Deposit date:
2012-12-19

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