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Structural studies of the polymorphs of carbamazepine, its dihydrate, and two solvates

Abstract:

High-field cross-polarisation magic-angle spinning 13C NMR spectra are presented for the four known polymorphe of anhydrous carbamazepine, for a dihydrate, and for two solvates. These are all distinctive, despite relatively low spectral dispersion, and give immediate information about the cristallographic asymmetric unit. The results for the trigonal and the two monoclinic forms are consistent with the published crystal structures. That of the triclinic form was found...

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Publication status:
Published

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Publisher copy:
10.1021/op0500990

Authors


Harris, RK More by this author
Puschmann, H More by this author
Apperley, DC More by this author
Griesser, UJ More by this author
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Journal:
ORGANIC PROCESS RESEARCH and DEVELOPMENT
Volume:
9
Issue:
6
Pages:
902-910
Publication date:
2005
DOI:
EISSN:
1520-586X
ISSN:
1083-6160
URN:
uuid:ff4911c8-6d14-496b-bdb2-7362764ffb3e
Source identifiers:
175630
Local pid:
pubs:175630
Language:
English

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