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A short and efficient synthesis of neodysiherbaine A by using catalytic oxidative cyclization.

Abstract:
To the point: The synthesis of the title compound was achieved with 24 overall yield through a sequence that has just seven linear steps (see scheme). Key points are the facial selectivity displayed by an oxocarbenium ion derived from a ribopyranose system and an osmium-catalyzed oxidative cyclization that is compatible with several acid-sensitive groups. Copyright © 2011 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim.
Publication status:
Published

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Publisher copy:
10.1002/anie.201102525

Authors


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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Organic Chemistry
Role:
Author
Journal:
Angewandte Chemie (International ed. in English) More from this journal
Volume:
50
Issue:
33
Pages:
7604-7606
Publication date:
2011-08-01
DOI:
EISSN:
1521-3773
ISSN:
1433-7851
Language:
English
Keywords:
Pubs id:
pubs:163943
UUID:
uuid:fc5bf706-9187-4cfe-b5e5-9acbe057e1a8
Local pid:
pubs:163943
Source identifiers:
163943
Deposit date:
2012-12-19

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