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Journal article

2-Azido-2-de-oxy-3,4-O-isopropyl-idene-2-C-methyl-d-talono-1,5-lactone.

Abstract:
The relative stereochemistry of the title compound, C(10)H(15)N(3)O(5), was confirmed by the crystal structure determin-ation. The absolute configuration was determined from the use of d-lyxonolactone as the starting material. The six-membered ring adopts a boat conformation with the larger azide group, rather than the methyl group, in the bowsprit position. In the crystal structure, a bifurcated inter-molecular O-H⋯O/O-H⋯N hydrogen bond links mol-ecules into chains running parallel to the b axis.
Publication status:
Published

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Publisher copy:
10.1107/s160053681001500x
Journal:
Acta crystallographica. Section E, Structure reports online More from this journal
Volume:
66
Issue:
Pt 5
Pages:
o1221-o1222
Publication date:
2010-01-01
DOI:
EISSN:
1600-5368
ISSN:
1600-5368
Language:
English
Pubs id:
pubs:54856
UUID:
uuid:fabf546e-d32f-46bd-b6f4-3b9ab51e3286
Local pid:
pubs:54856
Source identifiers:
54856
Deposit date:
2012-12-19

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