- Abstract:
-
We report a powerful new technique: hyphenating synchrotron X-ray powder diffraction (XRD) with differential scanning calorimetry (DSC). This is achieved with a simple modification to a standard laboratory DSC instrument, in contrast to previous reports which have involved extensive and complex modifications to a DSC to mount it in the synchrotron beam. The high-energy X-rays of the synchrotron permit the recording of powder diffraction patterns in as little as 2 s, meaning that thermally ind...
Expand abstract - Publication status:
- Published
- Peer review status:
- Peer reviewed
- Version:
- Accepted manuscript
- Files:
-
-
(pdf, 2.2MB)
-
- Publisher copy:
- 10.1021/acs.analchem.6b02549
-
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- Publisher:
- American Chemical Society Publisher's website
- Journal:
- Analytical Chemistry Journal website
- Volume:
- 88
- Issue:
- 20
- Pages:
- 10111-10117
- Publication date:
- 2016-09-05
- Acceptance date:
- 2016-09-19
- DOI:
- EISSN:
-
1520-6882
- ISSN:
-
0003-2700
- Pubs id:
-
pubs:648032
- URN:
-
uri:f99c7a8b-e86c-42e3-98c1-d27b0ea18fd6
- UUID:
-
uuid:f99c7a8b-e86c-42e3-98c1-d27b0ea18fd6
- Local pid:
- pubs:648032
- Language:
- English
- Keywords:
- Copyright holder:
- American Chemical Society
- Copyright date:
- 2016
- Notes:
- © 2016 American Chemical Society
Journal article
Simultaneous differential scanning calorimetry - synchrotron X-ray powder diffraction: A powerful technique for physical form characterisation in pharmaceutical materials.
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