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Simultaneous differential scanning calorimetry - synchrotron X-ray powder diffraction: A powerful technique for physical form characterisation in pharmaceutical materials.

Abstract:

We report a powerful new technique: hyphenating synchrotron X-ray powder diffraction (XRD) with differential scanning calorimetry (DSC). This is achieved with a simple modification to a standard laboratory DSC instrument, in contrast to previous reports which have involved extensive and complex modifications to a DSC to mount it in the synchrotron beam. The high-energy X-rays of the synchrotron permit the recording of powder diffraction patterns in as little as 2 s, meaning that thermally ind...

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Publication status:
Published
Peer review status:
Peer reviewed
Version:
Accepted manuscript

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Publisher copy:
10.1021/acs.analchem.6b02549

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Publisher:
American Chemical Society Publisher's website
Journal:
Analytical Chemistry Journal website
Volume:
88
Issue:
20
Pages:
10111-10117
Publication date:
2016-09-05
Acceptance date:
2016-09-19
DOI:
EISSN:
1520-6882
ISSN:
0003-2700
Pubs id:
pubs:648032
URN:
uri:f99c7a8b-e86c-42e3-98c1-d27b0ea18fd6
UUID:
uuid:f99c7a8b-e86c-42e3-98c1-d27b0ea18fd6
Local pid:
pubs:648032
Language:
English
Keywords:

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