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Layered double hydroxide nanosheets via solvothermal delamination

Abstract:

A new solvothermal post-synthesis treatment for preparing high aspect ratio magnesium aluminium layered double hydroxides (MgAl–LDHs) has been developed. Treating laurate-intercalated MgAl–LDHs in pure ethanol in an autoclave for 48 h at 150 °C was found to produce delaminated MgAl–LDH nanosheets with a thickness of ∼2.6 nm and an aspect ratio of ∼105. It is proposed that the high pressure solvothermal process promotes the insertion of ethanol molecules into the LDH interlayer space, thereby ...

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Publication status:
Published
Peer review status:
Peer reviewed

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Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
ORCID:
0000-0001-6610-8709
More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
ORCID:
0000-0003-2062-9546
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Oxford college:
Balliol College
Role:
Author
ORCID:
0000-0001-8054-8751
Publisher:
Elsevier
Journal:
Journal of Energy Chemistry More from this journal
Volume:
35
Pages:
88-94
Publication date:
2018-11-14
Acceptance date:
2018-11-06
DOI:
ISSN:
2095-4956
Language:
English
Keywords:
Pubs id:
pubs:950996
UUID:
uuid:f204bba8-c669-4c0b-b30e-9d1ee581fd36
Local pid:
pubs:950996
Source identifiers:
950996
Deposit date:
2019-03-25

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