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Journal article

tert-Butyl 2-de-oxy-4,5-O-isopropyl-idene-d-gluconate.

Abstract:
The relative configuration of tert-butyl 2-de-oxy-4,5-O-iso-propyl-idene-d-gluconate, C(13)H(24)O(6), an inter-mediate in the synthesis of 2-de-oxy sugars, was determined by X-ray crystallography, and the crystal structure consists of chains of O-H⋯O hydrogen-bonded mol-ecules running parallel to the a axis. There are two mol-ecules in the asymmetric unit. The absolute configuration was inferred from the use of d-erythrono-lactone as the starting material.
Publication status:
Published

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Publisher copy:
10.1107/s160053680803064x

Authors


Jenkinson, SF More by this author
Watkin, DJ More by this author
Journal:
Acta crystallographica. Section E, Structure reports online
Volume:
64
Issue:
Pt 10
Pages:
o2011-o2012
Publication date:
2008
DOI:
EISSN:
1600-5368
ISSN:
1600-5368
URN:
uuid:e6a7e0e2-ca16-44cc-8cae-a1b1bb43cb62
Source identifiers:
40911
Local pid:
pubs:40911
Language:
English

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