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Increasing the sensitivity of time-resolved photo-CIDNP experiments by multiple laser flashes and temporary storage in the rotating frame.

Abstract:

Pulse sequences have been developed that add up time-resolved photo-CIDNP signals from n successive laser flashes not in the acquisition computer of the NMR spectrometer but in the experiment itself, resulting in a greatly improved signal-to-noise ratio. For this accumulation, CIDNP is first stored in the transverse plane and then on the z axis, and finally superimposed on CIDNP produced by the next flash. These storage cycles also result in a very efficient background suppression. Because on...

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Publication status:
Published

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Publisher copy:
10.1016/j.jmr.2005.06.017

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Physical and Theoretical Chem
Journal:
Journal of magnetic resonance (San Diego, Calif. : 1997)
Volume:
177
Issue:
1
Pages:
139-145
Publication date:
2005-11-05
DOI:
EISSN:
1096-0856
ISSN:
1090-7807
URN:
uuid:e0ee2753-4242-402b-bf6b-84e85315157f
Source identifiers:
33212
Local pid:
pubs:33212

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