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Magnetic and microscopic investigation of airborne iron oxide nanoparticles in the London Underground

Abstract:
Particulate matter (PM) concentration levels in the London Underground (LU) are higher than London background levels and beyond World Health Organization (WHO) defined limits. Wheel, track, and brake abrasion are the primary sources of particulate matter, producing predominantly Fe-rich particles that make the LU microenvironment particularly well suited to study using environmental magnetism. Here we combine magnetic properties, high-resolution electron microscopy, and electron tomography to characterize the structure, chemistry, and morphometric properties of LU particles in three dimensions with nanoscale resolution. Our findings show that LU PM is dominated by 5–500 nm particles of maghemite, occurring as 0.1–2 μm aggregated clusters, skewing the size-fractioned concentration of PM artificially to larger sizes when measured with traditional monitors. Magnetic properties are largely independent of the PM filter size (PM10, PM4, and PM2.5), and demonstrate the presence of superparamagnetic (< 30 nm), single-domain (30–70 nm), and vortex/pseudo-single domain (70–700 nm) signals only (i.e., no multi-domain particles > 1 µm). The oxidized nature of the particles suggests that PM exposure in the LU is dominated by resuspension of aged dust particles relative to freshly abraded, metallic particles from the wheel/track/brake system, suggesting that periodic removal of accumulated dust from underground tunnels might provide a cost-effective strategy for reducing exposure. The abundance of ultrafine particles identified here could have particularly adverse health impacts as their smaller size makes it possible to pass from lungs to the blood stream. Magnetic methods are shown to provide an accurate assessment of ultrafine PM characteristics, providing a robust route to monitoring, and potentially mitigating this hazard.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1038/s41598-022-24679-4

Authors


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Institution:
University of Oxford
Division:
SSD
Department:
SOGE
Sub department:
Smith School
Role:
Author
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Role:
Author
ORCID:
0000-0002-2338-1219



Publisher:
Springer Nature
Journal:
Scientific Reports More from this journal
Volume:
12
Issue:
1
Article number:
20298
Place of publication:
England
Publication date:
2022-12-15
Acceptance date:
2022-11-18
DOI:
EISSN:
2045-2322
Pmid:
36522360


Language:
English
Keywords:
Pubs id:
1577510
Local pid:
pubs:1577510
Deposit date:
2023-12-05

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