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Uniform illumination of optically dense NMR samples.

Abstract:
We demonstrate a simple, inexpensive method for in situ laser illumination of NMR samples using a stepwise tapered optical fibre to deliver light uniformly along the axis of a 5 mm NMR tube. The optical path length of the incident light inside the sample is about 3 mm, allowing efficient illumination of optically dense samples. The degradation in spectral resolution and the reduction in filling factor are both minimal. Probe modifications are not required.
Publication status:
Published

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Publisher copy:
10.1016/j.jmr.2004.08.017

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Physical and Theoretical Chem
Journal:
Journal of magnetic resonance (San Diego, Calif. : 1997)
Volume:
171
Issue:
1
Pages:
171-175
Publication date:
2004-11-05
DOI:
EISSN:
1096-0856
ISSN:
1090-7807
URN:
uuid:d9bd3f62-c641-4e9d-9443-bca69a5ad7ce
Source identifiers:
32886
Local pid:
pubs:32886

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