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(2S,3R,4R,5S)-3,4-O-isopropylidene-2-methyl-1-oxa-6,9-diazaspiro[4.5]decane-7,10-dione

Abstract:
The synthesis of (2S,3R,4R,5S)-3,4-O-Isopropylidene-2-methyl-1-oxa-6,9- diazaspiro[4.5]decane -7,10-dione was investigated. The organic compound, C 11H13N2O5, was prepared from L-fucose in a sequence that produced this compound and an anomer. The crystal structure determination removed ambiguities in the synthetic sequence. The results show that the overall geometry is essentially same in the ordered and the disordered molecules and is unexceptional.
Publication status:
Published

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Publisher copy:
10.1107/S1600536804022494

Authors


Watkins, DJ More by this author
Bleriot, Y More by this author
Simone, MI More by this author
More by this author
Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Journal:
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
Volume:
60
Issue:
10
Pages:
O1820-O1822
Publication date:
2004-10-05
DOI:
EISSN:
1600-5368
ISSN:
1600-5368
URN:
uuid:d7d5a373-0029-450d-aa4d-207bff280fc8
Source identifiers:
39191
Local pid:
pubs:39191
Language:
English

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