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Time-resolved in situ neutron diffraction under supercritical hydrothermal conditions: a study of the synthesis of KTiOPO4.

Abstract:
In the first in situ neutron powder diffraction study of a supercritical hydrothermal synthesis, the crystallization of KTiOPO(4) (KTP) at 450 °C and 380 bar has been investigated. The time-resolved diffraction data suggest that the crystallization of KTP occurs by the reaction between dissolved K(+)(aq), PO(4)(3-)(aq), and [Ti(OH)(x)]((4-x)+)(aq) species.
Publication status:
Published

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Publisher copy:
10.1021/ja3088696

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Journal:
Journal of the American Chemical Society
Volume:
134
Issue:
43
Pages:
17889-17891
Publication date:
2012-10-05
DOI:
EISSN:
1520-5126
ISSN:
0002-7863
URN:
uuid:d13b30c6-b172-459e-8209-5b20b7724514
Source identifiers:
367962
Local pid:
pubs:367962
Language:
English

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