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Identifying suboxide grains at the metal–oxide interface of a corroded Zr–1.0%Nb alloy using (S)TEM, transmission-EBSD and EELS

Abstract:

Here we report a methodology combining TEM, STEM, Transmission-EBSD and EELS to analyse the structural and chemical properties of the metal–oxide interface of corroded Zr alloys in unprecedented detail. TEM, STEM and diffraction results revealed the complexity of the distribution of suboxide grains at the metal–oxide interface. EELS provided accurate quantitative analysis of the oxygen concentration across the interface, identifying the existence of local regi...

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Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1016/j.micron.2014.10.004

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Institution:
University of Oxford
Division:
MPLS
Department:
Materials
Role:
Author
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Westinghouse More from this funder
Rolls Royce More from this funder
China Scholarship Council More from this funder
Publisher:
Elsevier Publisher's website
Journal:
Micron Journal website
Volume:
69
Pages:
35-42
Publication date:
2014-10-29
Acceptance date:
2014-10-20
DOI:
ISSN:
0968-4328 and 1878-4291
Pmid:
25474748
Source identifiers:
492528
Language:
English
Keywords:
Pubs id:
pubs:492528
UUID:
uuid:cdeea896-681c-40ae-be19-d16f9d9fe890
Local pid:
pubs:492528
Deposit date:
2017-08-10

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