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A synchrotron radiation study of the hydrothermal synthesis of layered double hydroxides from MgO and Al2O3 slurries

Abstract:

The hydrothermal reaction of slurries containing MgO and Cp3 alumina has been investigated in situ using energy dispersive X-ray diffraction (EDXRD). A range of temperatures (100, 150, 180 and 240 °C) were studied. Kinetic data for the formation of the hydrotalcite-like Mg-Al layered double hydroxide (LDH) have been determined. At 100 °C the LDH is the predominant phase that is formed but at higher temperatures the impurity phases brucite and boehmite become more significant. The rate of reac...

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Publication status:
Published

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Publisher copy:
10.1039/b613795d

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Role:
Author
Journal:
GREEN CHEMISTRY
Volume:
9
Issue:
4
Pages:
373-378
Publication date:
2007-01-01
DOI:
EISSN:
1463-9270
ISSN:
1463-9262
URN:
uuid:bc54af8d-47c6-418a-b1dd-7011e922141b
Source identifiers:
51281
Local pid:
pubs:51281
Language:
English

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