- Abstract:
- The title compound 5,11,17,23-tetra-tert-butyl-N,N,-N′,N′-tetraethyl-26,28- dihydroxypentacyclo[19.3.1.13,7.-19,13.1 15,19]octacosa-1(25),3,5,7(26),9,11,13(27),15,17,-19(28),21,23- dodecaene-25,27-diylbis(oxythioacetamide), C56H78N2O4S2, was synthesized from the reaction of the known 1,3-bis(diethylamide)-substituted calix[4]-arene with 2,4-bis(4-methoxyphenyl)-1,3-dithia-2,4-diphosphetane-2,4-disulfide (Lawesson's reagent). The calixarene is found to have a pinched-cone conformation, with no solvent molecule in the cavity.
- Publication status:
- Published
- Publisher copy:
- 10.1107/S0108270196015521
-
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- Journal:
- ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
- Volume:
- 53
- Issue:
- 4
- Pages:
- 472-474
- Publication date:
- 1997-04-15
- DOI:
- ISSN:
-
0108-2701
- URN:
-
uuid:b715f7a2-3b52-4f25-b979-1ede35822f5f
- Source identifiers:
-
45508
- Local pid:
- pubs:45508
- Language:
- English
- Copyright date:
- 1997
Journal article
A calix[4]arene with diethylthiocarbamoylmethyloxy substituents in the 1,3 positions
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