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A calix[4]arene with diethylthiocarbamoylmethyloxy substituents in the 1,3 positions

Abstract:
The title compound 5,11,17,23-tetra-tert-butyl-N,N,-N′,N′-tetraethyl-26,28- dihydroxypentacyclo[19.3.1.13,7.-19,13.1 15,19]octacosa-1(25),3,5,7(26),9,11,13(27),15,17,-19(28),21,23- dodecaene-25,27-diylbis(oxythioacetamide), C56H78N2O4S2, was synthesized from the reaction of the known 1,3-bis(diethylamide)-substituted calix[4]-arene with 2,4-bis(4-methoxyphenyl)-1,3-dithia-2,4-diphosphetane-2,4-disulfide (Lawesson's reagent). The calixarene is found to have a pinched-cone conformation, with no solvent molecule in the cavity.
Publication status:
Published

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Publisher copy:
10.1107/S0108270196015521

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Role:
Author
Journal:
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
Volume:
53
Issue:
4
Pages:
472-474
Publication date:
1997-04-15
DOI:
ISSN:
0108-2701
URN:
uuid:b715f7a2-3b52-4f25-b979-1ede35822f5f
Source identifiers:
45508
Local pid:
pubs:45508
Language:
English

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