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Preparative HPLC separation of underivatized amino acids for isotopic analysis.

Abstract:

Single-compound analysis of stable or radio-isotopes has found application in a number of fields ranging from archaeology to forensics. Often, the most difficult part of these analyses is the development of a method for isolating the compounds of interest.Here, we describe three complementary preparative HPLC procedures suitable for separating and isolating single amino acids from bone collagen or hair keratin with minimal isotopic contamination. Using preparative reversed-phase, ion-pair, or...

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Volume:
828
Pages:
339-350
Publication date:
2012-01-01
DOI:
Source identifiers:
325077
ISBN:
9781617794445
Keywords:
Pubs id:
pubs:325077
UUID:
uuid:b62056d3-3820-4f8d-a696-f184545f2bd5
Local pid:
pubs:325077
Deposit date:
2012-12-20

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