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Crystal structure of [{(η7-C7H7)Mo(CO)2Ga}2(μ-OGaI3){μ- OGaI(OH)2}]2·3benzene

Abstract:

The crystal structure of [{(η7-C7H7)Mo(CO)2Ga}2(μ-OGaI3){μ-OGaI(OH)2}]2·3benzene has been obtained, revealing the following properties: triclinic, space group P1 with a = 11.191(2), b = 11.468(2), c = 15.913(3)Å, α = 77.18(3), β = 76.65(3), γ = 88.53(3)°, Z = 1, R = 0.030 and wR2 = 0.058 for 7870 observed reflections [I > 2σ(I)]. The coordination geometry about the molybdenum-bound gallium centres is approximately tetrahedral with a mean Mo-Ga distance of 2.541 Å and Mo-Ga-O angles of 122....

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Journal:
Analytical Sciences: X-ray Structure Analysis Online
Volume:
23
Issue:
4
Publication date:
2007-01-01
EISSN:
1348-2238
Source identifiers:
130684
Language:
English
Pubs id:
pubs:130684
UUID:
uuid:b6121288-dfe2-4ce2-a8c2-9df3d53b2239
Local pid:
pubs:130684
Deposit date:
2012-12-19

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