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One-pot cross-metathesis/tandem carbonyl ylide formation-intramolecular cycloaddition of an unsaturated 2-diazo-3,6-diketoester.

Abstract:
Dicarbonyl-stabilised diazo functionality is tolerated during alkene cross-metathesis using Grubbs' catalyst, but undergoes subsequent tandem carbonyl ylide formation-intramolecular 1,3-dipolar cycloaddition on addition of catalytic Rh2(OAc)4 in a one-pot operation.
Publication status:
Published

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Publisher copy:
10.1039/b515943a

Authors


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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Angrish, D More by this author
Labande, AH More by this author
Journal:
Chemical communications (Cambridge, England)
Volume:
6
Issue:
6
Pages:
627-628
Publication date:
2006-02-05
DOI:
EISSN:
1364-548X
ISSN:
1359-7345
URN:
uuid:aa931daa-f426-452a-bc48-426d47ca441c
Source identifiers:
33373
Local pid:
pubs:33373
Language:
English

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