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One-pot cross-metathesis/tandem carbonyl ylide formation-intramolecular cycloaddition of an unsaturated 2-diazo-3,6-diketoester.

Abstract:
Dicarbonyl-stabilised diazo functionality is tolerated during alkene cross-metathesis using Grubbs' catalyst, but undergoes subsequent tandem carbonyl ylide formation-intramolecular 1,3-dipolar cycloaddition on addition of catalytic Rh2(OAc)4 in a one-pot operation.
Publication status:
Published

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Publisher copy:
10.1039/b515943a

Authors


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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Organic Chemistry
Role:
Author
Journal:
Chemical Communications
Volume:
6
Issue:
6
Pages:
627-628
Publication date:
2006-02-01
DOI:
EISSN:
1364-548X
ISSN:
1359-7345
Source identifiers:
33373
Language:
English
Pubs id:
pubs:33373
UUID:
uuid:aa931daa-f426-452a-bc48-426d47ca441c
Local pid:
pubs:33373
Deposit date:
2012-12-19

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