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Exit wave reconstruction from focal series of HRTEM images, single crystal XRD and total energy studies on SbxWO3+y (x similar to 0.11)

Abstract:

A new tungsten bronze in the Sb-W-O system has been prepared in a solid state reaction from Sb 2O 3, WO 3 and W metal powder. The average structure was determined by single crystal X-ray diffraction. Sb xWO 3+y (x ~ 0.11) crystallizes in the orthorhombic space group Pm2 1n (no. 31), a = 27.8135(9)Å, b = 7.3659(2)Å and c = 3.8672(1)Å. The structure belongs to the (n)-ITB class of intergrowth tungsten bronzes. It contains slabs of hexagonal channels formed by six WO 6 octahedra. These slabs are...

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Publication status:
Published

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Publisher copy:
10.1524/zkri.2012.1517

Authors


Klingstedt, M More by this author
Sundberg, M More by this author
Eriksson, L More by this author
More by this author
Institution:
University of Oxford
Department:
Oxford, MPLS, Materials
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Journal:
ZEITSCHRIFT FUR KRISTALLOGRAPHIE
Volume:
227
Issue:
6
Pages:
341-349
Publication date:
2012
DOI:
ISSN:
0044-2968
URN:
uuid:9de45bd3-c463-4591-9132-c17af5bf28c3
Source identifiers:
356415
Local pid:
pubs:356415

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