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On the synthesis of pyrinodemin A. Part 1: The location of the olefin

Abstract:
The elucidation of the structure of the cytotoxic marine sponge alkaloid pyrinodemin A by synthesis is described. Based on the 13C NMR spectra of three double bond positional isomers and the natural product, it is concluded the C14′-C15′ isomer best represents the true structure of pyrinodemin A. In addition, the structural assignment of pyrinodemin C is evaluated. © 2004 Elsevier Ltd. All rights reserved.
Publication status:
Published

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Publisher copy:
10.1016/j.tet.2004.11.051

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Role:
Author
Journal:
TETRAHEDRON
Volume:
61
Issue:
5
Pages:
1127-1140
Publication date:
2005-01-31
DOI:
ISSN:
0040-4020
URN:
uuid:9cb6929a-e707-410c-a17c-ee1992a57e73
Source identifiers:
117895
Local pid:
pubs:117895
Language:
English
Keywords:

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