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The Synthesis and Crystal Structures of Two Hydrogen-Bonded N-Oxides

Abstract:

Abstract: (RS,RS,RS,RS)-3-(N-4′-Methoxyphenyl-N-methylamino)cyclohexane-1,2-diol N-oxide 10 and (1R,2S,3S,4R,7R,7aS,1′R)-1,2-dihydroxy-1,2-O-isopropylidene-3-(1′-hydroxy-2′-tert-butoxy-2′-oxoethyl)-7-(phenylthio)hexahydro-1H-pyrrolizine N(4)-oxide 14 were synthesised and studied by X-ray diffraction. The structure of 10·0.5CHCl3 crystallizes in the monoclinic space group P21/c with cell parameters of a = 22.8016(5) Å, b = 11.9666(2) Å, c = 11.6835(2) Å, β = 99.8698(9)°, V = 3140.75(10) Å3 and...

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Publication status:
Published

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Publisher copy:
10.1007/s10870-014-0549-8

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Role:
Author
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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Role:
Author
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Publisher:
Springer New York LLC
Journal:
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
Volume:
44
Issue:
11-12
Pages:
548-554
Publication date:
2014-12-05
DOI:
EISSN:
1572-8854
ISSN:
1074-1542
URN:
uuid:9947b177-64f0-4143-92a3-cd83c7e8e6cf
Source identifiers:
488981
Local pid:
pubs:488981
Language:
English
Keywords:

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