- Abstract:
-
As a method for the structure determination of integral membrane proteins or other large macromolecular complexes, a solid state 2H NMR approach is presented, capable of measuring the orientations of individual chemical bond vectors. In an immobilized uniaxially oriented sample, the bond angle of a deuterium-labelled methyl group relative to the axis of ordering can be calculated from the quadrupole splitting in the "zero-tilt" spectrum where the sample normal is aligned parallel to the spect...
Expand abstract - Publisher copy:
- 10.1016/0926-2040(93)90060-Z
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- Journal:
- Solid state nuclear magnetic resonance
- Volume:
- 2
- Issue:
- 1-2
- Pages:
- 21-36
- Publication date:
- 1993-04-05
- DOI:
- EISSN:
-
1527-3326
- ISSN:
-
0926-2040
- URN:
-
uuid:8d5ba8a3-a744-4d2b-9ff7-2064a6266ef4
- Source identifiers:
-
422167
- Local pid:
- pubs:422167
- Language:
- English
- Keywords:
- Copyright date:
- 1993
Journal article
2H NMR lineshapes of immobilized uniaxially oriented membrane proteins.
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